WebMay 1, 2008 · 2.. Results and discussionThe catalyst screen was run at relatively high catalyst loadings (substrate to catalyst molar ratio, S/C, of 50/1) and on a small scale (0.2. mmol of substrate for each reaction) using a parallel screening hydrogenation reactor Biotage Endeavor.. Time constraints and substrate availability limited the number of … WebHydrogenations (chiral/achiral) - Parr Reactors, Biotage Endeavor, and H.E.L. Cat96. Characterization - NMR, LC-MS, GC-MS (chiral and achiral), SFC, UPLC, DSC, TGA, SEC, UV-Vis. FT-IR, ReactIR, etc. Purification - column chromatography, prep-HPLC, recrystallization, liquid-liquid extraction, membrane chromatography, etc.

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Web10-position reaction station with 10-30 mL working volume, 400-2000 RPM stirring and heating. A larger 6-place parallel reaction station (reaction volumes up to 250 mL) is also available. Biotage Endeavor Pressure Reactor 8-position reaction station for high temperature and pressure work. WebNov 28, 2024 · To achieve high miscibility between these two fractions, three synthetic routes were investigated: mixtures of homogeneous catalysts, separately supported heterogeneous catalysts, and a co-anchoring strategy (CAS) to heterogenize different homogeneous catalysts on one solid support. WebBiotage hardware store st henry ohio